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Beilstein J. Org. Chem. 2020, 16, 670–673, doi:10.3762/bjoc.16.64
Graphical Abstract
Figure 1: Retrosynthetic analysis of chondrochlorene A (1).
Scheme 1: Synthesis of amide 3 [16-20]. TIPDSCl2 = 1,3-dichloro-1,1,3,3-tetraisopropyldisiloxane, TBSOTf = tert-buty...
Scheme 2: Synthesis of (Z)-bromide 4 using a palladium-catalyzed, stereoselective dehalogenation [21-24]. TBSOTf = t...
Scheme 3: Cross coupling of amide 3 and (Z)-bromide 4 (see Table 1 for conditions).